Dimethylthiocarbamoyl Chloride is an organosulfur compound, a yellow solid. It is often encountered as a yellow syrup. It is a key reagent in the synthesis of arylthiols via the Newman-Kwart rearrangement.
Dimethylthiocarbamoyl Chloride is prepared by chlorination of the related tetramethylthiuram disulfide: [Me2NC(S)]2S2 + 3 Cl2 → 2 Me2NC(S)Cl + 2 SCl. ) to give thiuram sulfides [R2NC(S)]2S. With methanethiolate, it gives methyl dimethyldithiocarbamate (Me2NC(S)SMe).
|Dimethylthiocarbamoyl chloride is used as an intermediate in the synthesis of pharmaceuticals.|
|It finds application in chemoselective deoxygenation of pyridine-N-oxides.|
|It is also used as a starting reagent in the synthesis of dimethylthiocarbamates.|
|Appearance||–||Yellow coloured solid|
|Melting Point||°C||40.5 – 43.5|
– Di Methyl Carbamoyl Chloride (DMCC)
– Other impurities
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